Chitosan — FTIR-absorptions-toppe og tildelinger
Dette er de karakteristiske FTIR-bølgetal, hvor Chitosan har tendens til at absorbere, samlet fra offentliggjort litteratur og rangeret efter understøttende evidens. Hver tildeling kan spores til en kilde (DOI) og er krydsvalideret mod vores 320,000+ referencespektrer og vidensgraf.
Understøttet af 8 citerede kilder
Hurtigt svar
Chitosan tildeles normalt ved at lede efter en tilbagevendende klynge af karakteristiske toppe frem for et præcist lærebogsnummer. Tabellen nedenfor viser, hvor litteraturen oftest placerer denne gruppe i FTIR, rangeret efter akkumuleret evidens.
Karakteristiske FTIR-toppe for Chitosan
| Bølgetal (cm⁻¹) | Understøttende fakta | Citerede kilder | Højeste tillid |
|---|---|---|---|
| 1655 | 4 | 4 | 1,0 |
| 1080 | 3 | 3 | 1,0 |
| 1642 | 3 | 2 | 1,0 |
| 1630 | 3 | 2 | 1,0 |
| 1062 | 2 | 2 | 1,0 |
| 1151 | 2 | 2 | 1,0 |
| 1610 | 2 | 2 | 1,0 |
| 1650 | 2 | 2 | 1,0 |
| 2800 | 2 | 2 | 1,0 |
| 3354 | 2 | 2 | 1,0 |
| 1418 | 2 | 2 | 1,0 |
| 3458 | 2 | 2 | 1,0 |
| 3000 | 2 | 2 | 1,0 |
| 1654 | 2 | 1 | 1,0 |
| 1452 | 1 | 1 | 1,0 |
| 2928 | 1 | 1 | 1,0 |
| 1012 | 1 | 1 | 1,0 |
| 1195 | 1 | 1 | 1,0 |
| 1106 | 1 | 1 | 1,0 |
| 1375 | 1 | 1 | 1,0 |
| 1705 | 1 | 1 | 1,0 |
| 2850 | 1 | 1 | 1,0 |
| 1633 | 1 | 1 | 1,0 |
| 1064 | 1 | 1 | 1,0 |
| 2874 | 1 | 1 | 1,0 |
| 1071 | 1 | 1 | 1,0 |
| 1148 | 1 | 1 | 1,0 |
| 3846 | 1 | 1 | 1,0 |
| 1230 | 1 | 1 | 1,0 |
| 3448 | 1 | 1 | 1,0 |
Viser de 30 bedst understøttede toppe ud af 148 i alt for Chitosan.
Spektrumlogik
En funktionel gruppetildeling bliver mere sikker, når flere forventede bånd optræder sammen. Brug denne side til at finde de bedst understøttede peaks, og bekræft derefter, at den samme prøve udviser et sammenhængende mønster snarere end et enkelt isoleret hit.
Anvendelse i virkeligheden
Disse sider er nyttige til analyse af ukendte materialer, topforklaring i rapporter, polymerfejlfinding og verifikation af, om en kandidatmaterialefamilie er kemisk plausibel.
Almindelige fejl
- Brug af én funktionel-gruppe-side som en komplet materialebedømmelse uden at kontrollere resten af spektret.
- Antager, at det stærkeste bånd altid er det mest diagnostiske.
- At glemme, at forarbejdning, tilsætningsstoffer, ældning og blandinger kan flytte eller udvide forventede toppe.
Verifikationsrådgivning
Brug DSC, GC-MS eller TGA, når flere materialefamilier deler lignende bånd, eller når blandings-effekter gør FTIR-tildelingen usikker.
Litteratur bag disse tildelinger
-
2361 cm⁻¹ tillid 1,0
“A signal at 1737 on chitosan spectrum was attributed to the carboxylic (C=O) groups T 2361cm-1 overlapped by MPEO incorporation.”
Mentha piperita essential oils loaded in a chitosan nanogel with inhibitory effect on biofilm formation against S. mutans on the dental surface DOI: 10.1016/j.carbpol.2019.02.018 -
2071 cm⁻¹ tillid 1,0
“3(b) that the introcm-1 the contact ion-pairs, the band at 2071 is attributed to the duction of the phthalimido group into the chitosan backbone has 2033cm-1 reflection triple ion aggregates and the band at is assigned to the disrupted the”
Synthesis and characterizations of phthaloyl chitosan-based polymer electrolytes DOI: 10.1016/j.jnoncrysol.2012.04.019 -
2908 cm⁻¹ tillid 1,0
“The peak at 2908.04 corresponded to cm(cid:2)1 Chitosan film CeH the stretching, while the band at 1335.74 was OeH the of water.”
Bourtoom 和 Chinnan - 2008 - Preparation and properties of rice starch-chitosan DOI: 10.1016/j.lwt.2007.10.014 -
2878 cm⁻¹ tillid 1,0
“The band at cm(cid:1)1 gelthestraincurvedisplaysajumpofthestrainvalueinresponse of chitosan corresponding to the C-H vibration, is 2878 OF cm(cid:1)1”
Improved mechanical and photophysical properties of chitosan incorporated folic acid gel possessing the characteristics of dye and metal ion absorption DOI: 10.1039/c2jm33995a -
3000 cm⁻¹ tillid 1,0
“Because the concentrated acids clean samples from any bands above 3000 are related to the overlap of the stretching impurity, which give chitosan more opportunities for recrystallization vibration of the OH and NH bonds [35, 36].”
A comparison of chitosan properties after extraction from shrimp shells by diluted and concentrated acids DOI: 10.1016/j.heliyon.2020.e03486 -
3438 cm⁻¹ tillid 1,0
“Figure 1C, for the hybrid brid chitosan-CuO nanocomposite, showed the noisy shape with the presence of the broad chitosan-CuO nanocomposite, showed the noisy shape with the presence of the broad band at 3438 cm-1 and the two characteristic”
Chitosan Capped Copper Oxide Nanocomposite: Efficient, Recyclable, Heterogeneous Base Catalyst for Synthesis of Nitroolefins DOI: 10.3390/catal12090964 -
3426 cm⁻¹ tillid 1,0
“Based on the FTIR spectra of the cm-1 chitosan membrane in Figure 2 showed that it has a wide absorption at 3425.58 that indicates the cm-1 vibration stretching -OH group.”
Synthesis and Characterization of Chitosan Membrane as a Matrix in Drug Delivery of Curcumin DOI: 10.1088/1757-899X/833/1/012068 -
3621 cm⁻¹ tillid 1,0
“FTIR spectrum presented significant peaks at 3621 1013 was attributed to chitosan, Accepted: 11October2022 cm-1 29Si, 27Al, 13H and 787 signified the stretching of Si-O-Si on HNT.”
Synthesis and Optimization of Superhydrophilic-Superoleophobic Chitosan–Silica/HNT Nanocomposite Coating for Oil–Water Separation Using Response Surface Methodology DOI: 10.3390/nano12203673
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